| Report | |
| Created on: | 1/14/2021 3:14:49 PM |
| Operator: | daq |
| File | |
| File name: | C:\XRD Data\QAQC\corundum 1_14_2021_SB.xrdml |
| Checksum: | 1F476825245D6F807E44DCCDC86805D2 |
| File size (bytes): | 46943 |
| Time stamp | |
| Started: | 1/14/2021 2:41:07 PM |
| Finished: | 1/14/2021 3:09:49 PM |
| Total time (h:m:s): | 00:28:42 |
| Status | |
| Completed | |
| Sample | |
| Sample type: | To be analyzed |
| Sample ID: | corundum 1_14_2021_SB |
| Measurement type | |
| Single scan | |
| Used wavelength | |
| Intended wavelength type: | Kα1 |
| Kα1 (Å): | 1.540598 |
| Kα2 (Å): | 1.544426 |
| Kα2/Kα1 intensity ratio: | 0.50 |
| Kα (Å): | 1.541874 |
| Kβ (Å): | 1.392250 |
| Incident beam path | |
| Radius (mm): | 145.0 |
| X-ray tube | |
| Name: | Empyrean Cu LFF HR (9430 033 7310x) DK424847 |
| Anode material: | Cu |
| Voltage (kV): | 40.0 |
| Current (mA): | 15.0 |
| Focus | |
| Focus type: | Line |
| Length (mm): | 12.0 |
| width (mm): | 0.4 |
| Take-off angle (°): | 6.0 |
| Soller slit | |
| Name: | Soller slits 0.04 rad. |
| Opening (rad.): | 0.04 |
| Mask | |
| Name: | Fixed mask 20 mm |
| Width (mm): | 16.00 |
| Divergence slit | |
| Name: | Divergence slit 1/4° |
| Distance to sample (mm): | 50 |
| Type: | Fixed |
| Height (mm): | 0.38 |
| Angle (°): | 0.2292 |
| Beam knife | |
| Name: | Beam knife high |
| Sample movement | |
| Movement type: | Spinning |
| Rotation time (s): | 1.0 |
| Diffracted beam path | |
| Radius (mm): | 145.0 |
| Anti-scatter slit | |
| Name: | AS slit 9 mm |
| Type: | Fixed |
| Height (mm): | 9.00 |
| Soller slit | |
| Name: | Large Soller slits 0.04 rad. |
| Opening (rad.): | 0.04 |
| Filter | |
| Name: | Large beta-filter Nickel |
| Thickness (mm): | 0.020 |
| Material: | Ni |
| Detector | |
| Name: | PIXcel1D-Medipix3 detector |
| Type: | RTMS detector |
| PHD - Lower level (keV): | 4.0 |
| PHD - Upper level (keV): | 11.3 |
| Mode: | Scanning |
| Active length (°): | 5.542 |
| Source | |
| Created by: | Instrument |
| Application SW: | Data Collector vs. 6.1a |
| Instrument control SW: | AERIS vs. 1.3.0 20191108 |
| Instrument ID: | 237972 |
| Sample mode | |
| Reflection | |
| Scan | |
| Start time stamp: | 1/14/2021 2:41:07 PM |
| End time stamp: | 1/14/2021 3:09:49 PM |
| Scan axis: | Gonio |
| Scan range (°): | 4.9900 - 120.0004 |
| Start position (°): | 4.9954 |
| End position (°): | 119.9950 |
| Step size (°): | 0.0109 |
| No. of points: | 10584 |
| Scan mode: | Continuous |
| Counting time (s): | 37.995 |