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User Guide Contents

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Topic

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Introduction

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Apparatus, Reagents, & Materials

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Instrument Calibration

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Sample Preparation

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Sample Analysis

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LIMS Integration

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Health, Safety, & Environment

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Maintenance & Troubleshooting

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The velocity logger measures ultrasonic sound speed in materials placed between its transducers in the x, y, and z-directions on working-half split core sections or discrete sample cubes (Figure 1). Minicores are measured in the x-direction, and cubes can be measured on any axis. Velocity data generated from these sensors are part of the physical properties suite of shipboard sample measurements.
For split core sections, velocity is measured in the x-direction using a caliper velocimeter and in the y- and z-directions using pairs of piezoelectric transducers. The laser measures the position of the top of the sample, and using this along with the offset to the transducers, calculates the position of the measurement in the sample (recorded as Offset in LIMS).
The caliper velocimeter measures velocity on discrete cubes in all three directions with no offset recorded.

Figure 1. Section Half Measurement Directions.

Method Theory

Measurement of P-wave velocity requires an estimate of the traveltime and an accurate measurement of the ultrasonic P-wave path length through the sample.
Velocity is defined as follows:
velocity = pathlength/traveltime, or
v = dS/dt.
Traveltime measurement is estimated by an algorithm for graphical first arrival pick. An ultrasonic pulser generates a high-impulse voltage, which is applied to the ultrasonic transmitter and thereby induces oscillation of the crystal element within the transducer-specific frequency band. A trigger pulse from the pulser is then applied to the oscilloscope to record the waveform from the receiving transducer.
By measuring the acoustic traveltime of the waveform through both specimen of the same material but variable thickness and instrumentation, linear regression through the dS/dt plot provides the instrumentation-specific time delay. Subtraction of the system delay time (+ liner material propagation time, if required) from the total traveltime gives the traveltime for the ultrasonic pulse through the sample.
Precise length of the sample is derived from the readout of a linear variable displacement transducer (LVDT). An AC linear variable differential transformer converts changes in physical position into an AC electrical output. The LVDT requires calibration, which is performed at the same time that the system delay is derived.
This LVDT functionality makes it mandatory that the system fully close the transducers when the software control program is opened and activated. Therefore, do not place a core section underneath the transducers when the software is started.
The chisel (bayonet) transducers are fixed at 8.2 cm for the z-axis (downhole) and 3.44 cm for the y-axis (IODP axis designation). The x-axis separation is derived from an LVDT and calibration constants.
Traveltimes for sample half sections are calculated as follows:
x-axis = total traveltime – x-system delay time – liner traveltime
y-axis = total traveltime – y-system delay time
z-axis = total traveltime – z-system delay time
Liner traveltime is calculated as the liner thickness (typically 2.7 mm) divided by the published liner material velocity (cellulose butyrate = 2140 m/s).

P-Wave Measurement

A temperature-equilibrated split core section in a half-core liner is placed on the core track. A barcode reader records all relevant sample information, which is used for the data upload into LIMS. A laser sensor measures the distance to the section end and determines the sampling interval from the difference between the position of the sensors and the end of the section. The user positions the section half under the sensor and triggers the measurement from the software control panel. The measurement is taken for a predetermined amount of time, generally 5 s, with the recorded result representing several thousand determinations.

Caliper Measurement

• The sample is placed between 2 flat, 1 inch diameter sensors that squeeze firmly onto the specimen to ensure good contact.
• One sensor acts as a transducer and the other as a receiver to record velocity measurements at a rate of 0.5 MHz.
• To measure discrete samples, the sample is measured along each (x, y, and z-) axis between the caliper sensors.
• A series of polycarbonate standards of different thickness are measured to obtain a linear regression transit time vs. distance for calibration. Their industry-calibrated standard sonic velocity is 2.750 m/s.

Bayonet Measurement

• Two pairs of piezoelectric transducers set at 90° to each other are inserted into the unconsolidated or semisoft section-half materials until the sensors are buried in the material to be measured.
• One of each pair of sensors acts as transducer and the other as receiver to measure velocity in two directions simultaneously.
• Calibration is performed by inserting the probes into a container filled with distilled water of known temperature, and therefore known velocity.

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• Quality of the acoustic coupling between the core material and the sensor transducers. Note: Use water to increase the quality of the contact.
• Quality of the coupling between both the transducer and the core liner and between the core liner and sample. Note: Use water to increase the quality of the contact.
• Consolidation of the sediments; noncohesive sediments containing microcracks or gas voids cannot be measured accurately.

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Apparatus, Reagents, & Materials

Hardware

The velocity track system consists of the following components (Figure 2):

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Figure 2. P-Wave Velocity Transducer Components.

Caliper Transducers: Panametrics-NDT Microscan Delay Line Transducers

Bayonet Transducers

Custom

Exlar Linear Actuator

Acuity 1000 Laser Distance Sensor

Microscan MS-4 Ultracompact Imager Barcode Reader

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Generally, only the marine technicians should access configurations settings in the velocity software. However, there are some configuration issues that users need to be aware of.
The program icon is shown in Figure 3. Double click to open and follow the prompts to display the program home screen. DO NOT place the sample below the instruments before opening the program, the program will close all transducers upon startup, and can cause severe injury.

Figure 3. Opening Program Desktop icon.

CAUTION: When first open the program, all 3 sensors will go through a communication initiation process where they will move down and up; the program will display a warning message first. However, make sure there are no samples or body parts underneath any of the sensors.
Figure 4, seen below, shows the home screen, which is the main program interface window. There are a number of graphical displays and adjustable settings. These are shown in detail on later figures.

Figure 4. Program home screen.

Configuration Editor: Station Setup Tab

The Station Setup tab (Figure 5) stores the physical configuration measurements of the caliper and bayonet transducers.

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Figure 5. Configuration Editor: Station Setup Tab.

Configuration Editor: DAQ Setup Tab

The DAQ Setup tab (Figure 6) stores settings for pick and arrival calculations.

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Figure 6. Configuration Editor: DAQ Setup Tab.

Caliper Calibration Tab

This tab (Figure 7) shows the results of the latest calibration and values used to calculate the calibration; values cannot be changed.

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Figure 7. Configuration Editor: Caliper Calibration Tab.

Bayonet Calibration Tab

This tab (Figure 8) shows the results of the latest bayonet calibration. Values cannot be changed.

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Figure 8. Configuration Editor: Bayonet Calibration Tab.

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VISA Resources Tab

This tab (Figure 9) shows the alias locations for the serial ports configured using LabView Measurement and Automation Explorer Program. Only Application Developers can change the values on this tab.
Figure 9. Configuration Editor: VISA Resources Tab.

File Paths Tab

This tab (Figure 10) shows the file paths used by the application to store the configuration file and data files. Only Application Developers can change the values on this tab.

Figure 10. Configuration Editor: File Paths Tab.

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• Laboratory reagent water (distilled)
• Aluminum cylinder of known length and velocity; velocity = 6295 m/s
• Acrylic (as above) half-cylinders of variable thicknesses to accommodate transducer placement on the half-core section. As of August 2010, the velocity is ~2950 m/s but subject to further verification.

Anchor_Ref302387099_Ref302387099
Figure 11. P-Wave Acrylic Cylinder Standards.

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Instrument Calibration

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The bayonet and caliper transducers must be calibrated and the system delay determined daily.

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Caliper calibration is a little bit more involved. Because the distance between the calipers is variable, the system delay is determined using a set of standards of identical velocity but various lengths. The actual velocity of the standard is irrelevant, but is good to know as a quality check. To determine the system delay time, the first arrival time is plotted against distance and the intercept with "zero distance" equals the system delay (Figure 17). As a quality check the the slope will equal the velocity of the material used. This value should be close to the known value and the r-value (fit) should equal 1 (or be very, very close). The calibration should look like the example shown below (note: the delay time will change as the transducers wear).

Figure 17. Caliper System Delay.
In addition to the delay time determination, the LVDT output (volts) must be calibrated to distance in millimeters (Figure 18). The known lengths of the same standards are used and both calibrations are performed at the same time. As standards are measured, the LVDT calibration improves, so previous measurements are constantly recalculated. This is one of the reasons why at least 6 measurements are required before accepting calibration.

Figure 18. LVDT Calibration.

Procedure

1. To begin calibration (Figure 19) to open the Caliper Calibration window for the PWV select the Caliper Piece X-Axis > then Stations > (Figure 20). to access the drop down menu, then > Calibrate Calipers.

Figure 19. Beginning a Caliper Calibration.

Figure 20. Caliper Calibration Window.
Enter the Aluminum width- 30 mm, place Aluminum Standard (30mm) on the transducer.
Close transducers slowly > Laser Offset (blue)
Aluminum Standard field should be 6295.00 > Determine System Delay (purple)
Adjust "threshold" until the redline on the graph is at first arrival point.
The Velocity should be very close to 6295.00, if so, then > Accept Changes.


Figure 21. Standard Information Dialog Box.

1. Place the cursor in the Scanner String field and scan the standard's 2D bar code. Once the information is automatically entered into the box, confirm the standard length and ensure the unit is meters. This value can be entered manually if necessary.
2. Place the standard in the caliper and click Start Measurement. During acquisition, the waveform, time pick, and calibration plots (after two measurements) will update on the Caliper Calibration window (Figure 22).

Figure 22. Standard Acquisition.

1. To stop the calibration, click the Stop – Return button on the Standard Information box (Figure 21). To resume measurement, click the Measure A Standard button on the Caliper Calibration window (Figure 22). To complete calibration, at least six standards must be measured; however, additional standards can be added or any standard can be measured multiple times.

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Calibration points can be edited if necessary. For example, the calibration curve in Figure 23 shows an obvious problem with one point: The wrong length was assigned to the standard.

Figure 23. Calibration Curve with an Error.

Procedure

1. Click the Stop – Return button on the Standard Identification box (Figure 21).
2. Locate the Index number of the point containing the wrong information on the Caliper Calibration screen and type it into the Index field (Figure 24).
3. Click Delete by Index to delete data for that point from the calibration.
4. Remeasure the standard using the Measure A Standard button.
5. Other options in the Array section of the Caliper Calibration screen include deleting only the last measurement (Delete Last) or deleting all data points and starting a new calibration (Delete All Data and Start Again) (Figure 24).

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To accept the calibration, click the Save button on the Caliper Calibration window (Figure 22).

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Sample Preparation

Two types of samples can be measured using the velocity gantry:

• Section-half core samples
• Discrete samples

Sample Prep Overview

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• Allow samples to equilibrate to room temperature before measuring velocity. \[Note: most samples will have already been run through the Whole-Round Multisensor Logger and will have been equilibrated to room temperature before that run.\]

  Before placing the working half in the core tray, make sure the surface is clean (lightly scrape away any material smeared across the cut surface during core splitting).
• Place the core section in the tray and make sure it is as flat as possible.

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• Clean transducers of any residue with water and paper towels.
• Before initializing the P-wave software, ensure the caliper transducers and laser beam are not blocked. Note: This step is crucial.

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Sample Analysis

Measuring Section-Half Samples

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Figure 25. Scan Sample Dialog Box.

1. Scan the barcode on the section half label to populate the fields on the Scan Sample Label dialog box. Enter Operator (user last name) and confirm measuring Station and Mode.

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1. For Section w/liner mode, a Position Sample dialog box opens (Figure 26). Confirm the sample position as measured by the laser (the laser at the end of the track measures the range to the end of the core and calculates the position in the liner based on an offset for that station). Click OK.

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Section-half measurements, in the liner. (X-Axis)Section-half measurements, in the liner. (X-Axis)Discrete sample (MAD cubes) measurements. (Z-Axis)Discrete sample (MAD cubes) measurements. (Y-Axis)Discrete sample (MAD cubes) measurements. (X-Axis)Piece measurements taken out of the section-half. Consolidated material only. (Any-Axis)Section-half measurements, in the liner. (X-Axis) Image Removed

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Figure 26. Position Sample Dialog Box.

1. The bayonet transducers lower into the section half; ensure they are completely inserted into the sample. If contact between the transducers and sediment is poor, add distilled water around the transducers to improve contact with sediment.
2. On the JOG Bayonet screen (Figure 27), monitor the waveform and position the transducer to obtain the best trace. The plot displays the live signal with no stacking. A weak signal is fine, as long as a clean first arrival is present. Once the waveform is acceptable, click Continue to begin sample acquisition.

Image AddedImage Removed
Figure 27. JOG Bayonet Y Screen.

1. During acquisition, the program adds multiple waveforms until the total (max peak) is greater than ±5 V. This process is repeated and the waveform is averaged.

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Figure 28. Scan Sample Label Dialog Box.

1. Scan the barcode on the discrete sample label to populate the fields on the Scan Sample Label screen. Enter Operator (user last name) and confirm measuring Station (Caliper) and Mode (Discrete).
2. Enter information requested in the Additional Discrete Information dialog box (Figure 29): Measurement Axis: X, Y, or Z.

Figure 29. Additional Discrete Information Dialog Box.

1. If the material to be measured is a whole piece removed from the liner (rarely used), select Piece w/o Liner mode in Step 4 and complete the offset (position of the piece in the liner before it was removed) in the Additional Piece Information dialog box (Figure 30).

If the orientation of the piece is unknown, check the Orientation Unknown box; otherwise the measurement is assigned to the X-direction.

Figure 30. Additional Piece Information Dialog Box.

1. Place the discrete sample in the caliper and add distilled water to create a good sample-transducer contact if needed.
2. On either the Additional Discrete Information (discrete samples) or Additional Piece Information (piece samples) box, select OK - AutoClose (for hard samples) or OK – Manual Close (for softer/friable samples).

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Figure 31. JOG Caliper Screen.

1. During acquisition, the program adds multiple waveforms until the total (max peak) is greater than ±5 V. This process is repeated and the waveform is averaged.

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Figure 33.A Manual Pick Screen. Anchor_GoBack_GoBack 

1. Click Continue to accept the manual pick and save it to the data file or Cancel to discard the manual pick results. AnchorRTF34343333393a204669675469RTF34343333393a204669675469

Data Handling

From the Display Results screen one of 4 data handling choices can be selected:

• Exit Save Data: saves data and returns to the Sample Information dialog box for the next sample.
• Cancel Without Saving Data: does not save the data but returns to the Sample Information dialog box. Use this option if there is a data quality warning or if the waveform for the sample was unacceptable.
• Repeat Without Saving Data and Keep ID: does not save data but returns to the JOG screen where the user can reposition the transducer and take another measurement of the same sample.
• Save Data and Repeat with Same ID: saves the data and returns to the JOG screen where the same sample can be run again. This option allows replicate measurements.

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LIMS Integration

Sample/Analysis Attributes and Components

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1. Open the LIMS Uploader icon on the desktop.
2. Click Start Monitoring to save data files and automatically upload calibration files to LIMS.
3. When data collection is completed, click Stop Monitoring.

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Health, Safety, & Environment

Safety

• Keep extraneous items and body parts away from the moving parts.
• The track system has a well-marked yellow and red emergency stop button (Figure 34) to halt the system if needed.
• Do not look directly into the laser light source (class 2 laser product).
• Do not direct the laser beam at other people.
• Do not attempt to work on the system while a measurement is in progress.
• Do not lean over or on the track.
• Do not stack anything on the track.
• This analytical system does not require personal protective equipment.

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AnchorRTF39323136383a204669675469RTF39323136383a204669675469 Image Removed
Anchor_Ref302387245_Ref302387245Figure 34. Emergency Stop Button.

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Maintenance & Troubleshooting

Common Issues

The following are common problems encountered when using the P-wave Velocity Gantry and their possible causes and solutions. For information about the laser Measurement and Operation software, see the Vp GIESA Gantry Laser Operation manual.

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The actuator utilities can be used to test the caliper and bayonet actuators (move them up and down) and view the waveform detected by the transducers. There are also utilities to test the home position of the actuators and to check the laser function. This utility is useful when configuring the station offsets.
To change the behavior and/or force of the actuators, the Exlar utility must be used.
Open the Actuator utility (Figure 35) from Main > Actuator Utility and then select one of the JOG screens, Home All, or Read Laser.

Figure 35. Actuator Utilities.

Scheduled Maintenance

After Every Sample

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