Before being crushed in the X-Press, hard rock samples for ICP analysis are polished (Figure 1.1 and 1.2) and cleaned in a sonic bath at least three times (for 10-15 minutes each): the first round of cleaning is with isopropyl alcohol and the following rounds are with DI water (Figure 1.3, see ICP Preparation for further details). Hard rock samples for XRD analysis do not usually need to be polished before being crushed.
Figure 1. Polishing and cleaning hard rock samples
Crushing Samples in the X-Press
The X-Press is a motorized hydraulic press that crushes hard rock and highly compacted sediment samples into smaller pieces.
Preparing the X-Press area
- First, clean the X-Press and counter with simple green and isopropyl alcohol. Lay down a Kimwipe or sheet of paper on the counter.
- Next collect the following supplies that make up the 'crushing unit' of the X-press (Figure 2). Materials are located in the drawer labeled 'X-PRESS SUPPLIES' in the X-Ray Prep Area in the Thin Section Lab.
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- Wearing nitrile gloves, wash the individual pieces of the grinding vessels with tap water and a small piece of a scouring pad (no soap). Rinse with DI water.
- After each piece is washed, dry it with a Kimwipe, immediately spray it with isopropyl alcohol, and wipe it down with a Kim Wipe. Do not use the ship's compressed air line to dry pieces as the air is too dirty.
- Lay the pieces on, and cover vessels with Kimwipes.
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